http://www.orgsyn.org/demo.aspx?prep=CV1P0186 WitrynaA solution of sodium ethoxide is prepared from 60 g. (2.6 gram atoms) of clean sodium and 700 cc. of absolute alcohol (Note 1) in a 2-l. round-bottomed flask equipped with a reflux condenser.To the hot solution is added a mixture of 234 g. (2 moles) of pure benzyl cyanide (Note 2) and 264 g. (3 moles) of dry ethyl acetate (Note 3).The mixture is …
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http://www.orgsyn.org/demo.aspx?prep=CV2P0047 WitrynaA solution of 50 g. of p-tolylsulfonylmethyl isocyanide in 150 ml. of dichloromethane is placed on a 40 × 3 cm. column containing about 100 g. of neutral alumina slurried in dichloromethane. A nearly colorless solution ( ca. 700 ml.) is collected over about 1 hour. This solution is evaporated to dryness on a rotary evaporator, providing 42 ... family holidays in the cotswolds
Organic Syntheses, Coll. Vol. 2, p.108 (1943); Vol. 16, p ...
WitrynaSłowa i wyrażenia podobne do słowa kościół. Lista słów i wyrażeń podobna do słowa kościół: kościół diecezjalny, kościół farny, kościół katedralny, kościół niebędący … WitrynaOrganic Syntheses, Inc., its Editors, and its Board of Directors do not warrant or guarantee the safety of individuals using these procedures and hereby disclaim any liability for any injuries or damages claimed to have resulted from or related in any way to the procedures herein. The paragraphs above were added in September, 2014. WitrynaIt melts at 65–71°. If pure ester is desired, it may be obtained by recrystallizing from petroleum ether (b.p. 70–90° ); the yield is 80–85 g. of ester melting at 74–75° from … family holidays in tenby wales